Imitego ya molekulari ya fosifora na reagent
Ibisobanuro ku bicuruzwa
Mu bizamini bya synthesis ya ABI na MilliGen / PerSeptive ADN, paki ya s-sieve irashobora kugumisha amazi mumacupa ya nitrile na activate munsi ya saa kumi za mugitondo, bitabaye ngombwa ko uhangayikishwa na valve cyangwa valve ya trottle igabanijwemo ibice.Umukungugu cyangwa linti kumufuka wapakiye urafunze.Irashobora gukoreshwa mu buryo butaziguye mu kuvoma amazi ya ml 500, 1L, 2 L hamwe n’andi macupa ya solve, kandi ibisobanuro bya paki ya s-sieve nabyo birashobora gutegurwa.
Ibikurikira byerekana ingaruka zingirakamaro zamazi yumutego wa 10 g mumutego wa 500ml, 1L, 4L ya nitrile hamwe nibirimo amazi atandukanye.
Gereranya numutego utumizwa mu mahanga
| 500 ml 197 ppm ACN | |||||
| Igihe (h) | 0 | 24 | 48 | 72 | 96 |
| HonyaBio | 197 | 33 | 16.5 | 6.5 | 6 |
| Ibindi bihugu | 197 | 43 | 27 | 15 | 15 |
| 1 L 143 ppm ACN | |||||
| Igihe (h) | 0 | 24 | 48 | 72 | 96 |
| HonyaBio | 143 | 48 | 32 | 20 | 15 |
| Ibindi bihugu | 142 | 47 | 36 | 23 | 15 |
| 4 L 141 ppm ACN | |||||
| Igihe (h) | 0 | 24 | 48 | 72 | 96 |
| HonyaBio | 141 | 95 | 94 | 84 | 73 |
| Ibindi bihugu | 141 | 96 | 95 | 85 | 72 |
Amabwiriza n'imikoreshereze
Umutego wa molekuline urimo vacuum, kandi ugomba gukingurwa niyo wakoreshwa, kandi kashe ya icupa rya reagent igomba gukingirwa mugihe cyo kuyikoresha.
Amashanyarazi ya 2g kuri 24 h arashobora kugabanya 165 ppm yamazi muri ml 500 nitrile kugeza 105 ppm.
Amashanyarazi 5 g kuri 24 h arashobora kugabanya 172 ppm y'amazi muri 500 ml nitrile kugeza 58 ppm.
10 g gushungura 24 h Irashobora kugabanya 166 ppm y'amazi muri 1 L nitrile kugeza 68 ppm.
20 g sub-sieve irashobora kugabanya 162 ppm y'amazi muri nitrile 4 L kugeza 109 ppm kuri 24 h.
Turasaba 2 g kugabanura amacupa ya reagent ya 50-250ml, 5g kumacupa ya reagent 250-500ml, 10g kumacupa ya reagent 500-1000ml, na 20g kumacupa ya reagent 1000-2000ml.
Ibyiringiro
Buri sub-ecran yamashanyarazi igenzurwa neza mugihe cyibikorwa.Kandi birakenewe ko abakiriya bagenzura ibipfunyika mbere yo gukoresha:
Ubwa mbere, wemeze ko icyuho cyo gupakira kituzuye.Icyuho cyose gisohoka cyangwa ikirere cyinjira bizagabanya imikorere yibicuruzwa.
Icya kabiri, witondere mugihe ufunguye ibipfunyika kugirango wirinde ko sub-ecran yapakira firime idashushanywa, hanyuma urebe niba film ihari Hano harasohoka.
Kuvura nyuma yo gukoreshwa
Ntabwo ari uburozi cyangwa ngo byangiza, bizanduzwa n’imiti n’umuti bahura nabyo kandi bigomba kujugunywa nkimyanda yanduye nyuma yo kuyikoresha.
Icyitegererezo na Porogaramu
Twabanje gutanga imifuka yo munsi yubunini bwa 2 g, 5 g, 10 g, na 20 g., Nibindi bisobanuro birashobora gutegurwa ukurikije ibyo abakiriya bakeneye.
Umutego wa molekuline urakwiriye guhura na nitrile igihe kirekire, kandi ushobora no gukoreshwa kuri acide acetike, ether, ether acetike, butyl acetate, inzoga, isopropanol, methanol, butanol, Phenol, pyridine, aside hydrochloric, aside nitric, aside fosifori , aside sulfurike, methyl chloride, azote methyl imidazole, nibindi
Ntishobora kuba ikwiriye guhura nigihe kirekire na tetrahydrofuran, toluene, methyl formamide (DMF), methyl methyl amide (DMAc), N-methylpyrrolidone (NMP) nibindi bisubizo.
